The photo electric effect

Nearly all types of electromagnetic radiation can be used for spectroscopy to study and characterise matter. When using X-rays the photoelectric effect occurs. 

The photoelectric effect refers to the emission or ejection of electrons from the surface of a sample in response to electromagnetic radiation or light. Energy contained within the electromagnetic radiation is absorbed by electrons within the sample, giving the electrons sufficient energy to be 'knocked' out of (emitted from) the sample. 

In the X-ray region atoms absorb X-rays sharply at certain wavelengths (called absorption edges) that are characteristic of that particular atomic species. So if you shine a particular frequency or energy of X-rays onto a sample, you can control the type of electron that is emitted.

XAS Graph c_1256x1056

Different Types of XAS techniques

X-ray Absorption Near Edge Structure (XANES) refers to the absorption fine structure close to an absorption edge, about 10 eV below the absorption edge and 20 eV above the edge. This region usually shows the largest variations in the X-ray absorption coefficient and is often dominated by intense, narrow resonances. This part of the spectrum provides information on the electronic structure of the unoccupied levels and the geometry of the studied element - very few techniques can do this.   

XANES is also referred to as Near Edge X-Ray Absorption Fine Structure (NEXAFS). Today, the term NEXAFS is typically used for soft X-ray absorption spectra (surface science, organics) and XANES for hard X-ray spectra (coordination chemistry, metal atoms).  

EXAFS is the part of XAS spectrum - typically starting ~ 50 eV above the absorption edge. It originates from the scattering of a photoelectron ejected from the absorbing atom and its neighbours. EXAFS is therefore typically used to determine the local structure of the studied element and its surrounding atoms.

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